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用简单的溶液燃烧法合成NiMO双金属催化剂,并以CH4为碳源采用化学气相沉积法(CVD)制备合成高质量碳纳米管;考察了催化剂组成、制备温度、CH4流速对CVD制备碳纳米管的影响;采用XRD、Raman、SEM、TEM等手段对合成的催化剂和碳纳米管进行了表征。该实验将前沿的科学研究成果转化融入实验教学,介绍了常见的纳米材料合成与表征的相关知识,进行了CVD碳纳米管合成参数优化,旨在引导学生从本质上理解合成参数对碳纳米管生长的影响,培养学生的科研思维,激发学生的研究兴趣。
Abstract：NiMo bimetallic catalyst is synthesized by the simple solution combustion method, and high quality carbon nanotubes are synthesized by chemical vapor deposition(CVD) with CH4 as carbon source. The effects of catalyst composition, preparation temperature and CH4 flow rate on the preparation of carbon nanotubes by CVD are investigated, and the catalyst and carbon nanotubes are characterized by means of XRD, Raman, SEM, TEM, etc. In this experiment, the cutting-edge scientific research results are integrated into the experimental teaching, and the common knowledge about the synthesis and characterization of nano materials is introduced. In order to guide students to understand the effect of synthesis parameters on the growth of carbon nanotubes, the optimization of synthesis parameters of CVD carbon nanotubes is carried out, which is helpful to cultivate students' scientific research thinking and stimulate their research interest.
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基本信息:
DOI：10.16791/j.cnki.sjg.2021.05.037
中图分类号:TB383.1-4;G642.423;O613.71-4
引用信息:
[1]柯丁宁,宋琳琳,况婷.化学气相沉积法制备碳纳米管的材料化学综合实验设计[J].实验技术与管理,2021,38(05):180-186.DOI:10.16791/j.cnki.sjg.2021.05.037.
基金信息:
广东省高等教育高水平大学建设计划项目（AZ11000098）; 哈尔滨工业大学（深圳）创新实验课建设项目（INEP1021）
2020-09-26
2020
2020-10-13
2020
1
2021-05-20
2021-05-20
2021-05-20